Diamond anvils alignment

Good anvil alignment is needed for making reliable gaskets (proper pre-indentation and hole centring) and to ensure successful experiments. This page describes the steps to follow for diamond anvils alignment for a DAC.
Before starting the alignment
- Check that the anvils are properly fixed in their supports;
- Verify that all screws are correctly tightened;
- Ensure both anvils are clean and free of debris (dust, metal particles, old gasket material).
Lateral alignment of the anvils
- Bring the upper anvil close to the lower one, but do not put them in contact;
- Observe both culets under the microscope;
- Use the cell lateral screws to adjust the lower side anvil so the culets appear concentric;
- The goal is to see two culets that overlap perfectly when viewed from above.
The video on the right shows an example on how to adjust the lateral alignment on a HeliosDAC diamond anvil cell.
Tilt alignment
- Carefully bring the anvils in contact and observe the interference fringe pattern;
- Note the point where the fringes are densest => one needs to adjust the anvil position in this area.
- Note the DAC orientation, so as not to worsen the alignment with the adjustment (both X and Y directions are reversed under the metallurgical microscope);
- Increase the distance between the anvils;
- Use the DAC’s tilt screws to adjust the anvil position:
- Tighten the screw (or screws) in the area where the fringes are densest. Tightening a screw pulls the anvil support up, thus increasing the diamonds separation. To be able to tighten the screw, one needs first to loosen the two opposite screws;
- Repeat the above steps until only 3-4 large colored fringes are obtained.
Watch the video on the right for more tips on how to fine-tune the tilt alignment.
What good alignment looks like
- Perfect overlap of culets;
- No more than 3-4 wide colored fringes;
-
Uniform pre-indentation mark on both sides of the gasket;
-
Sample hole centered on both side of the gasket.
Signs of misalignment
- Crescent shadows on one side;
- Multitude of colored narrow fringes;
- Off-center hole on one side of the gasket and centered on the other side;
- Early anvils failure or gasket failure.
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